methyl 4-acetamidobenzenesulfinate

Base Information

Chemical Name:methyl 4-acetamidobenzenesulfinate
CAS No.:958814-70-5
Molecular Formula:C₉H₁₁NO₃S
Molecular Weight:213.257
Hs Code.:

Synonyms:methyl 4-acetamidobenzenesulfinate

Suppliers and Price of methyl 4-acetamidobenzenesulfinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-acetamidobenzenesulfinate

Chemical Property:

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Technology Process of methyl 4-acetamidobenzenesulfinate

There total 3 articles about methyl 4-acetamidobenzenesulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67-56-1
methanol

: 1126-81-4
4-acetamidothiophenol

: 958814-70-5
methyl 4-acetamidobenzenesulfinate

Guidance literature:: With oxygen; potassium carbonate; at 60 ℃; for 24h; chemoselective reaction; Schlenk technique;
DOI:10.1039/c8gc00441b

Reference yield: 56.0%

: 67-56-1
methanol

: 3989-50-2
4-acetamidobenzenesulfonylhydrazine

: 958814-70-5
methyl 4-acetamidobenzenesulfinate

Guidance literature:: With sodium hydrogensulfite; at 80 ℃; for 6h; Schlenk technique; Green chemistry;
DOI:10.1002/adsc.202001202

Reference yield:

: 121-60-8
p-acetylaminobenzenesulfonyl chloride

: 958814-70-5
methyl 4-acetamidobenzenesulfinate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / tetrahydrofuran / 0 °C / Inert atmosphere

2: sodium hydrogensulfite / 6 h / 80 °C / Schlenk technique; Green chemistry

With hydrazine hydrate; sodium hydrogensulfite; In tetrahydrofuran;
DOI:10.1002/adsc.202001202