8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide

Base Information

Chemical Name:8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide
CAS No.:135980-26-6
Molecular Formula:C₂₈H₄₈N₄O₄
Molecular Weight:504.714
Hs Code.:

Synonyms:8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide

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Chemical Property of 8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide

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Technology Process of 8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide

There total 7 articles about 8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135980-25-5
(5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid benzyl ester

: 135980-26-6
8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 0.666667h; under 1551.4 Torr; Ambient temperature;

Reference yield:

: 6850-57-3
2-methoxybenzylamine

: 135980-26-6
8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) ethyl chlorocarbonate, Et₃N, / 1. CHCl₃, 0 deg C, 30 min, 2.) CHCl₃

2: 6 g / H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

3: 1.) ethyl chlorocarbonate, Et₃N, / 1. CHCl₃, 0 deg C, 30 min, 2.) CHCl₃

4: H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

5: 1.) ethyl chlorocarbonate, Et₃N, / 1. dioxane, 0 deg C, 30 min, 2.) dioxane

6: H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In methanol;

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 135980-26-6
8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) ethyl chlorocarbonate, Et₃N, / 1. CHCl₃, 0 deg C, 30 min, 2.) CHCl₃

2: 6 g / H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

3: 1.) ethyl chlorocarbonate, Et₃N, / 1. CHCl₃, 0 deg C, 30 min, 2.) CHCl₃

4: H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

5: 1.) ethyl chlorocarbonate, Et₃N, / 1. dioxane, 0 deg C, 30 min, 2.) dioxane

6: H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In methanol;