(5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester

Base Information

Chemical Name:(5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester
CAS No.:135980-27-7
Molecular Formula:C₃₁H₅₂N₄O₆
Molecular Weight:576.777
Hs Code.:

Synonyms:(5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester

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Chemical Property of (5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester

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Technology Process of (5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester

There total 8 articles about (5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 541-41-3
chloroformic acid ethyl ester

: 135980-26-6
8-(6-Amino-hexanoylamino)-octanoic acid [5-(2-methoxy-benzylcarbamoyl)-pentyl]-amide

: 135980-27-7
(5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester

Guidance literature:: With pyridine; In chloroform; at 0 ℃; for 3h;

Reference yield:

: 6850-57-3
2-methoxybenzylamine

: 135980-27-7
(5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) ethyl chlorocarbonate, Et₃N, / 1. CHCl₃, 0 deg C, 30 min, 2.) CHCl₃

2: 6 g / H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

3: 1.) ethyl chlorocarbonate, Et₃N, / 1. CHCl₃, 0 deg C, 30 min, 2.) CHCl₃

4: H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

5: 1.) ethyl chlorocarbonate, Et₃N, / 1. dioxane, 0 deg C, 30 min, 2.) dioxane

6: H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

7: 51 percent / pyridine / CHCl₃ / 3 h / 0 °C

With pyridine; hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In methanol; chloroform;

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 135980-27-7
(5-{7-[5-(2-Methoxy-benzylcarbamoyl)-pentylcarbamoyl]-heptylcarbamoyl}-pentyl)-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) ethyl chlorocarbonate, Et₃N, / 1. CHCl₃, 0 deg C, 30 min, 2.) CHCl₃

2: 6 g / H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

3: 1.) ethyl chlorocarbonate, Et₃N, / 1. CHCl₃, 0 deg C, 30 min, 2.) CHCl₃

4: H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

5: 1.) ethyl chlorocarbonate, Et₃N, / 1. dioxane, 0 deg C, 30 min, 2.) dioxane

6: H₂ / 10percent Pd/C / methanol / 0.67 h / 1551.4 Torr / Ambient temperature

7: 51 percent / pyridine / CHCl₃ / 3 h / 0 °C

With pyridine; hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In methanol; chloroform;