5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione

Base Information

Chemical Name:5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione
CAS No.:144460-15-1
Molecular Formula:C₁₅H₁₈N₂OS
Molecular Weight:274.387
Hs Code.:

Synonyms:5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione

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Technology Process of 5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione

There total 3 articles about 5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 144460-14-0
5-acetyl-3,4-dimethyl-6-phenyl-3,6-dihydro-2(1H)pyrimidinethione

: 77-78-1
dimethyl sulfate

: 144460-15-1
5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione

Guidance literature:: In methanol; for 3h; Heating;
DOI:10.1246/bcsj.65.2246

Reference yield:

: 100-52-7
benzaldehyde

: 144460-15-1
5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 2 M HCl / methanol; H₂O / 24 h / Ambient temperature

2: 60 percent / methanol / 3 h / Heating

With hydrogenchloride; In methanol; water;
DOI:10.1246/bcsj.65.2246

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 144460-15-1
5-acetyl-3,4-dimethyl-6-phenyl-2-methylthio-3,6-dihydro-2(1H)pyrimidinethione

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 2 M HCl / methanol; H₂O / 24 h / Ambient temperature

2: 60 percent / methanol / 3 h / Heating

With hydrogenchloride; In methanol; water;
DOI:10.1246/bcsj.65.2246