FMOC-L-METHIONYL CHLORIDE

Base Information

Chemical Name:FMOC-L-METHIONYL CHLORIDE
CAS No.:103321-54-6
Molecular Formula:C20H20 Cl N O3 S
Molecular Weight:389.9
Hs Code.:
Mol file:103321-54-6.mol

Synonyms:Carbamicacid, [(1S)-1-(chlorocarbonyl)-3-(methylthio)propyl]-, 9H-fluoren-9-ylmethylester (9CI); Carbamic acid, [1-(chlorocarbonyl)-3-(methylthio)propyl]-,9H-fluoren-9-ylmethyl ester, (S)-

Suppliers and Price of FMOC-L-METHIONYL CHLORIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
FMOC-L-METHIONYL CHLORIDE 95.00%
5MG
$ 501.56

Total 2 raw suppliers

Chemical Property of FMOC-L-METHIONYL CHLORIDE

Chemical Property:

PSA：80.70000
LogP:4.80310
Storage Temp.:Store at 0°C

Purity/Quality:

98%Min ^*data from raw suppliers

FMOC-L-METHIONYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of FMOC-L-METHIONYL CHLORIDE

There total 3 articles about FMOC-L-METHIONYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.3%

: 71989-28-1
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-methionine

: 103321-54-6
Fmoc-methioninechloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jo00369a042

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 103321-54-6
Fmoc-methioninechloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 50 °C

2: thionyl chloride / dichloromethane / 4 h / 50 °C / Inert atmosphere

With thionyl chloride; sodium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 63-68-3,26062-47-5,58576-49-1
L-methionine

: 103321-54-6
Fmoc-methioninechloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 50 °C

2: thionyl chloride / dichloromethane / 4 h / 50 °C / Inert atmosphere

With thionyl chloride; sodium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;