(2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

Base Information

Chemical Name:(2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester
CAS No.:124931-83-5
Molecular Formula:C₂₉H₂₂O₄
Molecular Weight:434.491
Hs Code.:

Synonyms:(2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

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Chemical Property of (2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

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Technology Process of (2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

There total 1 articles about (2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 93-25-4
2-methoxyphenylacetic acid

: 18531-99-2
(S)-[1,1']-binaphthalenyl-2,2'-diol

: 124931-83-5
(2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 4h; Ambient temperature;

Reference yield:

: 75-30-9
2-iodo-propane

: 124931-83-5
(2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

: (S)-2-(2-Methoxy-phenyl)-3-methyl-butyric acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 15 min, 2.) THF, -78 deg C, 8.0 h;

Reference yield:

: 513-38-2
Isobutyl iodide

: 124931-83-5
(2-Methoxy-phenyl)-acetic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

: (S)-2-(2-Methoxy-phenyl)-4-methyl-pentanoic acid 2'-hydroxy-[1,1']binaphthalenyl-2-yl ester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 15 min, 2.) THF, from -78 deg C to -55 deg C, 9.5 h;