(12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)acetic acid, methyl ester of

Base Information

• Chemical Name: (12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)acetic acid, methyl ester of
• CAS No.: 910449-80-8
• Molecular Formula: C₂₇H₃₆N₄O₇
• Molecular Weight: 528.605

Synonyms:(12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)acetic acid, methyl ester of

Chemical Property of (12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)acetic acid, methyl ester of

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of (12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)acetic acid, methyl ester of

There total 3 articles about (12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)acetic acid, methyl ester of which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene (910449-79-5) + bromoacetic acid methyl ester (96-32-2) → (12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1(14),11(15),12-trien-3-yl)acetic acid, methyl ester of (910449-80-8)

Guidance literature:

With potassium carbonate; In acetonitrile; for 18h; Reflux;

Reference yield:

3-HYDROXYPYRIDINE (109-00-2) → (12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1(14),11(15),12-trien-3-yl)acetic acid, methyl ester of (910449-80-8)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium hydroxide / water / 20 - 90 °C

2: potassium carbonate / acetonitrile / 12 h / Reflux

3: carbon tetrabromide; triphenylphosphine / acetonitrile / 6 h / 5 - 20 °C

4: potassium carbonate / acetonitrile / 2 h / Reflux

5: mercaptoacetic acid; lithium hydroxide / N,N-dimethyl-formamide / 20 °C

6: potassium carbonate / acetonitrile / 18 h / Reflux

With carbon tetrabromide; potassium carbonate; mercaptoacetic acid; triphenylphosphine; sodium hydroxide; lithium hydroxide; In water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

2,6-bis-(hydroxymethyl)-3-hydroxypyridine (38029-16-2) → (12-benzyloxy-6,9-bis(methoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1(14),11(15),12-trien-3-yl)acetic acid, methyl ester of (910449-80-8)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium carbonate / acetonitrile / 12 h / Reflux

2: carbon tetrabromide; triphenylphosphine / acetonitrile / 6 h / 5 - 20 °C

3: potassium carbonate / acetonitrile / 2 h / Reflux

4: mercaptoacetic acid; lithium hydroxide / N,N-dimethyl-formamide / 20 °C

5: potassium carbonate / acetonitrile / 18 h / Reflux

With carbon tetrabromide; potassium carbonate; mercaptoacetic acid; triphenylphosphine; lithium hydroxide; In N,N-dimethyl-formamide; acetonitrile;

upstream raw materials:

3-HYDROXYPYRIDINE

12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene

bromoacetic acid methyl ester

2,6-bis-(hydroxymethyl)-3-hydroxypyridine

Downstream raw materials:

(12-Benzyloxy-6,9-bis(carboxymethyl)-3,6,9,15-tetraazabicyclo[9.3.1]-pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)acetic acid

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