12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid

Base Information

Chemical Name:12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid
CAS No.:149183-56-2
Molecular Formula:C₃₃H₅₁F₃N₂O₄S₂
Molecular Weight:660.906
Hs Code.:

Synonyms:12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid

Suppliers and Price of 12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid

There total 9 articles about 12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128886-88-4
4-<3-trifluoromethyl-3H-diazirin-3-yl>benzaldehyde

: 82001-53-4
12-mercaptododecanoic acid

: 149183-56-2
12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 1h; Yield given;
DOI:10.1021/ja00062a009

Reference yield:

: 82001-53-4
12-mercaptododecanoic acid

: 149183-55-1
3-(4-(2-(1,3-dioxanyl))phenyl)-3-(trifluoromethyl)diazirine

: 149183-56-2
12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 1h; Yield given;
DOI:10.1021/ja00062a009

Reference yield:

: 1-(4-(2-(1,3-dioxanyl))phenyl)-2,2,2-trifluoro-1-ethanone oxime

: 149183-56-2
12-{(11-Carboxy-undecylsulfanyl)-[4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-methylsulfanyl}-dodecanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / triethylamine (TEA), 4-(dimethylamino)pyridine (DMAP) / CH₂Cl₂ / Ambient temperature

2: 70 percent / ammonia (liquid) / diethyl ether; CHCl₃ / 12 h / Ambient temperature

3: 73 percent / triethylamine (TEA), iodine / methanol / 1 h

4: boron trifluoride etherate / CH₂Cl₂ / 1 h / 0 °C

With dmap; boron trifluoride diethyl etherate; ammonia; iodine; triethylamine; In methanol; diethyl ether; dichloromethane; chloroform;
DOI:10.1021/ja00062a009