N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

Base Information

Chemical Name:N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide
CAS No.:157734-20-8
Molecular Formula:C₂₀H₂₆N₂O₃S
Molecular Weight:374.504
Hs Code.:

Synonyms:N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

Suppliers and Price of N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

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Chemical Property of N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

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Technology Process of N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

There total 1 articles about N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96-09-3
styrene oxide

: 76867-83-9
N-(p-tolyl)methanesulfonimidomorpholide

: 157734-20-8
N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) ether, hexane, RT, 30 min, 2.) ether, hexane, 12 h;
DOI:10.1246/bcsj.67.1855

Reference yield: 91.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 157734-20-8
N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

: 157734-21-9
C₂₆H₄₀N₂O₃SSi

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 45 ℃; for 48h;
DOI:10.1246/bcsj.67.1855

Reference yield:

: 157734-20-8
N-(p-tolyl)-3-hydroxy-3-phenylpropanesulfonimidomorpholide

: C₂₇H₄₃N₂O₃SSi⁽¹⁺⁾*CF₃O₃S^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / imidazole / dimethylformamide / 48 h / 45 °C

2: CH₂Cl₂ / 72 h

With 1H-imidazole; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.67.1855