2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride

Base Information

Chemical Name:2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride
CAS No.:134767-75-2
Molecular Formula:C₁₇H₁₅ClN₂O₂*ClH
Molecular Weight:351.232
Hs Code.:

Synonyms:2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride

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Chemical Property of 2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride

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Technology Process of 2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride

There total 5 articles about 2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 134767-66-1
4-Amino-3-[2-(2-chloro-phenyl)-acetylamino]-benzoic acid ethyl ester

: 134767-75-2
2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride

Guidance literature:: With hydrogenchloride; zinc(II) chloride; In ethanol; for 3h; Heating;
DOI:10.1002/ardp.19913240505

Reference yield:

: 51512-09-5
2-(2-chlorophenyl)acetyl chloride

: 134767-75-2
2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / benzene / 3 h / Heating

2: 38 percent / ZnCl₂, HCl(g) / ethanol / 3 h / Heating

With pyridine; hydrogenchloride; zinc(II) chloride; In ethanol; benzene;
DOI:10.1002/ardp.19913240505

Reference yield:

: 2444-36-2
2'-chloro-benzeneacetic acid

: 134767-75-2
2-(2-chlorophenyl)methyl-5-<1H>benzimidazole carboxylic acid ethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / benzene / 1 h / 80 °C

2: pyridine / benzene / 3 h / Heating

3: 38 percent / ZnCl₂, HCl(g) / ethanol / 3 h / Heating

With pyridine; hydrogenchloride; thionyl chloride; zinc(II) chloride; In ethanol; benzene;
DOI:10.1002/ardp.19913240505