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Technology Process of H3BP(C6H5)((CH2)14)

H3BP(C6H5)((CH2)14)

Base Information
  • Chemical Name:H3BP(C6H5)((CH2)14)
  • CAS No.:709008-47-9
  • Molecular Formula:C20H36BP
  • Molecular Weight:318.291
  • Hs Code.:
H<sub>3</sub>BP(C<sub>6</sub>H<sub>5</sub>)((CH<sub>2</sub>)14)

Synonyms:H3BP(C6H5)((CH2)14)

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Chemical Property of H3BP(C6H5)((CH2)14)
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Technology Process of H3BP(C6H5)((CH2)14)

There total 1 articles about H3BP(C6H5)((CH2)14) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

H<sub>3</sub>BP(C<sub>6</sub>H<sub>5</sub>)((CH<sub>2</sub>)6CHCH(CH<sub>2</sub>)6)

H3BP(C6H5)((CH2)6CHCH(CH2)6)

hydrogen
1333-74-0

hydrogen

H<sub>3</sub>BP(C<sub>6</sub>H<sub>5</sub>)((CH<sub>2</sub>)14)
709008-47-9

H3BP(C6H5)((CH2)14)

Guidance literature:
Wilkinson's catalyst; In benzene; charging of Fischer-Porter bottle with H3BP(Ph)((CH2)6CHCH(CH2)6), Rh(PPh3)3Cl and benzene, flushing with H2; stirring under H2 (6 atm) for 20 h; removal of solvent by oil-pump vac., chromy. on neutral alumina using 1:1 v/v CH2Cl2-hexanes; removal of solvent by oil-pump vac., as oil; elem.anal.;
DOI:10.1039/b400156g

Reference yield: 24.0%

[(μ-chloro)2(tetrahydrothiophene)2(pentafluorophenyl)2(platinum(II))2]
77347-62-7

[(μ-chloro)2(tetrahydrothiophene)2(pentafluorophenyl)2(platinum(II))2]

H<sub>3</sub>BP(C<sub>6</sub>H<sub>5</sub>)((CH<sub>2</sub>)14)
709008-47-9

H3BP(C6H5)((CH2)14)

trans-[Pt(Cl)(C<sub>6</sub>F<sub>5</sub>)(PPh(CH<sub>2</sub>)14)2]
709008-48-0

trans-[Pt(Cl)(C6F5)(PPh(CH2)14)2]

Guidance literature:
With HNEt2; In dichloromethane; byproducts: PPh(CH2)14; (N2); charging of Schlenk flask with H3BPPh(CH2)14 and HNEt2; stirring at 50°C for 45 min; removal of HNEt2 (vac.), drying (vac.) at 50°C for 20 min; repeat twice (2 h; 50°C); addn. of (PtClC6F5SC4H8)2 and CH2Cl2; stirring for 16 h; removal of solvent by oil-pump vac., chromy. on neutral alumina using 1:1 v/v CH2Cl2-hexanes; removal of solvent by oil-pump vac., as oil; solidifying over the course of several days; elem. anal.;
DOI:10.1039/b400156g
upstream raw materials:

hydrogen

Downstream raw materials:

trans-[Pt(Cl)(C6F5)(PPh(CH2)14)2]

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