3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Base Information

Chemical Name:3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical
CAS No.:215956-73-3
Molecular Formula:C₁₅H₁₈NO₂S
Molecular Weight:276.379
Hs Code.:

Synonyms:3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

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Chemical Property of 3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

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Technology Process of 3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

There total 1 articles about 3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108-98-5
thiophenol

: 85591-99-7
3-bromo-4-formyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

: 215956-73-3
3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; for 1h; Ambient temperature;
DOI:10.1055/s-1998-2178

Reference yield: 75.0%

: 215956-73-3
3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

: 215956-75-5
3-(hydroxymethyl)-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 0.5h; Ambient temperature;
DOI:10.1055/s-1998-2178

Reference yield:

: 215956-73-3
3-formyl-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

: 215956-77-7
3-(bromomethyl)-2,2,5,5-tetramethyl-4-phenylthio-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NaBH₄ / ethanol / 0.5 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

3: LiBr / acetone / 0.5 h / Heating

With sodium tetrahydroborate; triethylamine; lithium bromide; In ethanol; dichloromethane; acetone;
DOI:10.1055/s-1998-2178