C₂₂H₁₄N₄O₄

Base Information

Chemical Name:C₂₂H₁₄N₄O₄
CAS No.:1309659-71-9
Molecular Formula:C₂₂H₁₄N₄O₄
Molecular Weight:398.378
Hs Code.:

C<sub>22</sub>H<sub>14</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₂₂H₁₄N₄O₄

Suppliers and Price of C₂₂H₁₄N₄O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₁₄N₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₁₄N₄O₄

There total 6 articles about C₂₂H₁₄N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18511-71-2
4,4'-dibromo-2,2'-bipyridine

: 190788-59-1
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nitrobenzene

: 1309659-71-9
C₂₂H₁₄N₄O₄

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; water; toluene; for 24h; Reflux;

Reference yield:

: 366-18-7
[2,2]bipyridinyl

: 1309659-71-9
C₂₂H₁₄N₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 12 h / -78 - 20 °C

2: nitric acid; sulfuric acid / 12 h / 80 °C

3: Acetyl bromide / acetic acid / 3 h / 40 °C

4: phosphorus tribromide / chloroform / 2 h / -3 - 60 °C / Inert atmosphere

5: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; tetrahydrofuran / 24 h / Reflux

With Acetyl bromide; sulfuric acid; nitric acid; phosphorus tribromide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; chloroform; water; acetic acid; toluene;

Reference yield:

: 577-19-5
2-nitrophenyl bromide

: 1309659-71-9
C₂₂H₁₄N₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate / [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / toluene / 10 h / Reflux

2: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; tetrahydrofuran / 24 h / Reflux

With potassium acetate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); In tetrahydrofuran; water; toluene;