Pyridine, 4-[(2-propenyloxy)methyl]- (9CI)

Base Information

• Chemical Name: Pyridine, 4-[(2-propenyloxy)methyl]- (9CI)
• CAS No.: 102547-80-8
• Molecular Formula: C₉H₁₁NO
• Molecular Weight: 149.192
• Mol file: 102547-80-8.mol

Synonyms:Pyridine,4-[(2-propenyloxy)methyl]- (9CI); Pyridine, 4-[(allyloxy)methyl]- (6CI)

Chemical Property of Pyridine, 4-[(2-propenyloxy)methyl]- (9CI)

Chemical Property:

• Boiling Point: 94 - 96 °C (5 mmHg)
• PSA: 22.12000
• LogP: 1.78420

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pyridine, 4-[(2-propenyloxy)methyl]- (9CI)

There total 2 articles about Pyridine, 4-[(2-propenyloxy)methyl]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

4-bromomethyl pyridine hydrobromide (73870-24-3,1119106-77-2) + allyl alcohol (107-18-6) → 4-((allyloxy)methyl)pyridine (102547-80-8)

Guidance literature:

With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; at 20 ℃;

DOI:10.1002/anie.201912119

Reference yield:

sodium allyloxide (20907-32-8) + 4-picolylchloride hydrochloride (1822-51-1) → 4-((allyloxy)methyl)pyridine (102547-80-8)

Guidance literature:

With allyl alcohol;

Reference yield:

4-((allyloxy)methyl)pyridine (102547-80-8) → (RS)-1-(4-pyridyl)but-3-en-1-ol (17285-59-5,144635-04-1,517907-58-3)

Guidance literature:

With sodium amide; xylene;

upstream raw materials:

sodium allyloxide

4-picolylchloride hydrochloride

4-bromomethyl pyridine hydrobromide

allyl alcohol

Downstream raw materials:

(RS)-1-(4-pyridyl)but-3-en-1-ol