(E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:(E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide
CAS No.:1284229-97-5
Molecular Formula:C₂₇H₃₁N₃O₃S
Molecular Weight:477.627
Hs Code.:

Synonyms:(E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide

Suppliers and Price of (E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide

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Technology Process of (E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide

There total 3 articles about (E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1284230-07-4
2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexanone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1284229-97-5
(E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide

Guidance literature:: In diethyl ether; at 20 ℃; for 12h;
DOI:10.1002/anie.201006996

Reference yield:

: 4894-75-1
1-phenyl-4-cyclohexanone

: 1284229-97-5
(E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: rac-Pro-OH / water; dimethyl sulfoxide / 2.5 h / 46 °C / Microwave irradiation

2: diethyl ether / 12 h / 20 °C

With rac-Pro-OH; In diethyl ether; water; dimethyl sulfoxide; 1: Mannich reaction;
DOI:10.1002/anie.201006996

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1284229-97-5
(E)-N'-{2-[(4-methoxyphenylamino)methyl]-4-phenylcyclohexylidene}-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: rac-Pro-OH / water; dimethyl sulfoxide / 2.5 h / 46 °C / Microwave irradiation

2: diethyl ether / 12 h / 20 °C

With rac-Pro-OH; In diethyl ether; water; dimethyl sulfoxide; 1: Mannich reaction;
DOI:10.1002/anie.201006996