(S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

Base Information

Chemical Name:(S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester
CAS No.:126228-87-3
Molecular Formula:C₄₀H₃₇N₅O₁₀
Molecular Weight:747.761
Hs Code.:

Synonyms:(S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

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Chemical Property of (S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

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Technology Process of (S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

There total 3 articles about (S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 62625-24-5
4-(Phenylazo)phenacyl bromide

: (S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid 4-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

: 126228-87-3
(S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

Guidance literature:: With triethylamine; In acetone; for 0.5h; Ambient temperature;
DOI:10.1055/s-1989-27312

Reference yield:

: (S)-2-Amino-succinic acid 4-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

: 126228-87-3
(S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / methanol / 0.08 h / Ambient temperature

2: 80 percent / Et₃N / acetone / 0.5 h / Ambient temperature

With potassium hydroxide; triethylamine; In methanol; acetone;
DOI:10.1055/s-1989-27312

Reference yield:

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 126228-87-3
(S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / methanol / 0.08 h / Ambient temperature

2: 80 percent / Et₃N / acetone / 0.5 h / Ambient temperature

With potassium hydroxide; triethylamine; In methanol; acetone;
DOI:10.1055/s-1989-27312