(S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide

Base Information

Chemical Name:(S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide
CAS No.:126046-22-8
Molecular Formula:BrH*C₃₂H₂₇N₅O₆
Molecular Weight:658.508
Hs Code.:

Synonyms:(S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide

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Chemical Property of (S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide

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Technology Process of (S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide

There total 4 articles about (S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 126228-87-3
(S)-2-(2,2-Bis-ethoxycarbonyl-vinylamino)-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

: 126046-22-8
(S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide

Guidance literature:: With bromine; In chloroform; Ambient temperature;
DOI:10.1055/s-1989-27312

Reference yield:

: 62625-24-5
4-(Phenylazo)phenacyl bromide

: 126046-22-8
(S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Et₃N / acetone / 0.5 h / Ambient temperature

2: 70 percent / 4percent Br₂ / CHCl₃ / Ambient temperature

With bromine; triethylamine; In chloroform; acetone;
DOI:10.1055/s-1989-27312

Reference yield:

: (S)-2-Amino-succinic acid 4-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester

: 126046-22-8
(S)-2-Amino-succinic acid bis-[2-oxo-2-(4-phenylazo-phenyl)-ethyl] ester; hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / methanol / 0.08 h / Ambient temperature

2: 80 percent / Et₃N / acetone / 0.5 h / Ambient temperature

3: 70 percent / 4percent Br₂ / CHCl₃ / Ambient temperature

With potassium hydroxide; bromine; triethylamine; In methanol; chloroform; acetone;
DOI:10.1055/s-1989-27312