C₃₆H₄₄ClFN₂O₅

Base Information

Chemical Name:C₃₆H₄₄ClFN₂O₅
CAS No.:1335557-68-0
Molecular Formula:C₃₆H₄₄ClFN₂O₅
Molecular Weight:639.207
Hs Code.:

C<sub>36</sub>H<sub>44</sub>ClFN<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₆H₄₄ClFN₂O₅

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Chemical Property of C₃₆H₄₄ClFN₂O₅

Chemical Property:

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Technology Process of C₃₆H₄₄ClFN₂O₅

There total 11 articles about C₃₆H₄₄ClFN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1335557-67-9
C₃₆H₄₅FN₂O₆

: 1335557-68-0
C₃₆H₄₄ClFN₂O₅

Guidance literature:: With dmap; methanesulfonyl chloride; triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 220901-72-4
3-fluoro-6-methoxy-2-methylbenzoic acid

: 1335557-68-0
C₃₆H₄₄ClFN₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

1.2: 12 h / 25 °C

2.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

3.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

4.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

5.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

7.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

7.2: 0.5 h / -78 °C

7.3: -78 - 20 °C

8.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

9.1: tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate / acetonitrile / 24 h / 70 °C

10.1: dmap; triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 20 °C

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; tetrabutylammomium bromide; water; nitric acid; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; methanesulfonyl chloride; triethylamine; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; In tetrahydrofuran; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 394-04-7
5-fluoro-2-methoxybenzoic acid

: 1335557-68-0
C₃₆H₄₄ClFN₂O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 2 h / -78 °C

1.2: 2 h / -78 - 25 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

2.2: 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

5.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

6.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

7.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

8.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

8.2: 0.5 h / -78 °C

8.3: -78 - 20 °C

9.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

10.1: tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate / acetonitrile / 24 h / 70 °C

11.1: dmap; triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 20 °C

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; water; sec.-butyllithium; nitric acid; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; methanesulfonyl chloride; triethylamine; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; In tetrahydrofuran; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile;