N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide)

Base Information

• Chemical Name: N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide)
• CAS No.: 949572-56-9
• Molecular Formula: C₇₄H₇₈N₂O₈
• Molecular Weight: 1123.44
• Mol file: 949572-56-9.mol

Synonyms:N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide)

Chemical Property of N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide)

There total 6 articles about N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

N,N'-dipentyl-1,6,7,12-tetrachloroperylene-3,4:9,10-bis(dicarboximide) (696601-54-4) + para-tert-butylphenol (98-54-4) → N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide) (949572-56-9)

Guidance literature:

With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 130 ℃; for 14h; Inert atmosphere;

DOI:10.1002/chem.200800156

Reference yield: 34.0%

ethanolamine (141-43-5) + n-Pentylamine (110-58-7) + 1,6,7,12-tetrakis(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid dianhydride (156028-30-7) → N-2'-hydroxyethyl-N'-pentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide) (862100-52-5) + C68H66N2O10 + N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide) (949572-56-9)

Guidance literature:

In toluene; Reflux;

DOI:10.1002/chem.200800156

Reference yield:

n-Pentylamine (110-58-7) → N,N'-dipentyl-1,6,7,12-tetra(p-tert-butylphenoxy)perylene-3,4:9,10-bis(dicarboximide) (949572-56-9)

Guidance literature:

Multi-step reaction with 2 steps

1: propionic acid / Reflux

2: potassium carbonate / 1-methyl-pyrrolidin-2-one / 14 h / 130 °C / Inert atmosphere

With potassium carbonate; propionic acid; In 1-methyl-pyrrolidin-2-one;

DOI:10.1002/ejoc.201100513

upstream raw materials:

N,N'-dipentyl-1,6,7,12-tetrachloroperylene-3,4:9,10-bis(dicarboximide)

para-tert-butylphenol

ethanolamine

n-Pentylamine

Downstream raw materials:

1,6,7,12-tetrakis(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid dianhydride