1,3-Diallyl-5,6-diaminouracil hydrochloride

Base Information

• Chemical Name: 1,3-Diallyl-5,6-diaminouracil hydrochloride
• CAS No.: 102284-74-2
• Molecular Formula: C10H14 N4 O2
• Molecular Weight: 0
• Mol file: 102284-74-2.mol

Synonyms:2,4(1H,3H)-Pyrimidinedione,5,6-diamino-1,3-di-2-propenyl- (9CI); 1,3-Diallyl-5,6-diaminouracil; 5,6-Diamino-1,3-diallyluracil

Chemical Property of 1,3-Diallyl-5,6-diaminouracil hydrochloride

Chemical Property:

• PSA: 96.04000
• LogP: 0.70880

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Diallyl-5,6-diaminouracil hydrochloride

There total 2 articles about 1,3-Diallyl-5,6-diaminouracil hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1,3-diallyl-6-amino-5-nitrosouracil (102284-73-1) → 1,3-diallyl-5,6-diaminouracil (102284-74-2)

Guidance literature:

With ammonium hydroxide; sodium dithionite; In water;

DOI:10.1021/jm00157a035

Reference yield:

1,3-diallyl-6-aminouracil (4852-19-1) → 1,3-diallyl-5,6-diaminouracil (102284-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / NaNO₂, HCl / acetic acid; methanol; H₂O / 0.25 h

2: 70 percent / aq. 50percent NH₄OH, Na₂S₂O₄ / H₂O

With hydrogenchloride; ammonium hydroxide; sodium dithionite; sodium nitrite; In methanol; water; acetic acid;

DOI:10.1021/jm00157a035

Reference yield: 75.0%

(E)-1,3-diallyl-6-amino-5-(3,4,5-trimethoxycinnamoyl)aminouracil (142665-25-6) + (E)-3,4,5-trimethoxy-cinnamic acid (20329-98-0,20329-99-1,90-50-6) + 1,3-diallyl-5,6-diaminouracil (102284-74-2) → (E)-1,3-Diallyl-8-(3,4,5-trimethoxystyryl)xanthine (142665-35-8)

Guidance literature:

upstream raw materials:

1,3-diallyl-6-amino-5-nitrosouracil

1,3-diallyl-6-aminouracil

Downstream raw materials:

(E)-1,3-Diallyl-8-(3,4,5-trimethoxystyryl)xanthine

4-(2,3,6,7-tetrahydro-2,6-dioxo-1,3-di-2-propenyl-1H-purine-8-yl)benzenesulfonic acid

N-[3-(dimethylamino)propyl]-4-(2,3,6,7-tetrahydro-2,6-dioxo-1,3-di-2-propenyl-1H-purine-8-yl)benzenesulfonamide

(E)-1,3-Diallyl-8-(3,4-dimethoxystyryl)xanthine