methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

Base Information

Chemical Name:methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate
CAS No.:173097-65-9
Molecular Formula:C₂₀H₂₂O₅
Molecular Weight:342.392
Hs Code.:

Synonyms:methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

Chemical Property:

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Technology Process of methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

There total 3 articles about methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 173097-64-8
(4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylic acid

: 74-88-4
methyl iodide

: 173097-65-9
methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; for 48h; Ambient temperature;
DOI:10.1002/hlca.19950780703

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 173097-65-9
methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg / 2.) THF, 1 h, 20-30 deg C

2: 93 percent / Na₂CO₃ / dimethylformamide / 48 h / Ambient temperature

With sodium carbonate; magnesium; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19950780703

Reference yield:

: 67844-12-6
methyl (4S,5S)-2,2-dimethyl-1,3-dioxolane-4-carboxylic acid-5-carboxylate

: 173097-65-9
methyl (4S,5S)-5-(hydroxydiphenylmethyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg / 2.) THF, 1 h, 20-30 deg C

2: 93 percent / Na₂CO₃ / dimethylformamide / 48 h / Ambient temperature

With sodium carbonate; magnesium; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19950780703