6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

Base Information

Chemical Name:6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose
CAS No.:951165-32-5
Molecular Formula:C₆₆H₇₄O₁₇Si₂
Molecular Weight:1195.47
Hs Code.:

Synonyms:6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

Suppliers and Price of 6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of 6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

There total 1 articles about 6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₅₀O₁₁Si₂

: 98-88-4
benzoyl chloride

: 951165-32-5
6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

Guidance literature:: In pyridine; at 20 ℃;
DOI:10.1016/j.carres.2007.05.009

Reference yield: 72.0%

: 951165-32-5
6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

: 142386-46-7
2,3,4,2',3',4'-hexakis-O-benzoyl-α,α-D-trehalose

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; acetic acid; for 24h;
DOI:10.1016/j.carres.2007.05.009

Reference yield:

: 951165-32-5
6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

: 951165-34-7
2,3,4,6,2',3',4'-hepta-O-benzoyl-6'-O-phenoxythiocarbonyl-α,α-D-trehalose

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / TBAF / tetrahydrofuran; acetic acid / 24 h

2: DMAP / pyridine / 12 h / 20 °C

3: 140 mg / DMAP / acetonitrile

With dmap; tetrabutyl ammonium fluoride; In tetrahydrofuran; pyridine; acetic acid; acetonitrile;
DOI:10.1016/j.carres.2007.05.009