bis (p-toluene sulfonamide) dimesitylgermane

Base Information

Chemical Name:bis (p-toluene sulfonamide) dimesitylgermane
CAS No.:200729-46-0
Molecular Formula:C₃₂H₃₈GeN₂O₄S₂
Molecular Weight:651.387
Hs Code.:

Synonyms:bis (p-toluene sulfonamide) dimesitylgermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis (p-toluene sulfonamide) dimesitylgermane

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Technology Process of bis (p-toluene sulfonamide) dimesitylgermane

There total 2 articles about bis (p-toluene sulfonamide) dimesitylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 96481-42-4
dichlorodimesitylgermane

: 70-55-3
toluene-4-sulfonamide

: 200729-46-0
bis (p-toluene sulfonamide) dimesitylgermane

Guidance literature:: With triethylamine; In tetrahydrofuran; byproducts: Et3N*HCl; inert atmosphere; addn. of Ge-compd. to mixt. of 1 equiv. of sulfonamideand excess Et3N, stirring (room temp., 3 h); concn., filtration off of Et3N*HCl at 0°C, evapn. (room temp.); elem. anal.;
DOI:10.1016/S0022-328X(97)00449-X

Reference yield:

: 96481-42-4
dichlorodimesitylgermane

: 70-55-3
toluene-4-sulfonamide

: 200729-41-5
N-dimesitylchlorogermyl p-toluene sulfonamide

: 200729-46-0
bis (p-toluene sulfonamide) dimesitylgermane

Guidance literature:: With triethylamine; In tetrahydrofuran; byproducts: Et3N*HCl; inert atmosphere; addn. of excess Et3N to equimolar amts. of sulfonamideand Ge-compd., stirring (room temp., 2 h); filtration off of Et3N*HCl, evapn. (vac.), washing (ether), drying (vac.);
DOI:10.1016/S0022-328X(97)00449-X