5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester

Base Information

Chemical Name:5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester
CAS No.:363602-35-1
Molecular Formula:C₂₃H₂₅NO₆
Molecular Weight:411.455
Hs Code.:

Synonyms:5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester

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Chemical Property of 5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester

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Technology Process of 5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester

There total 4 articles about 5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 100-39-0
benzyl bromide

: 363602-34-0
5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl ester

: 363602-35-1
5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1021/ol016158l

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 363602-35-1
5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 98 percent / sodium hydroxide / H₂O; dioxane / 0 - 20 °C

2.1: NaHCO₃ / dimethylformamide

2.2: 34 percent / dimethylformamide / 24 h

3.1: 81 percent / NaHCO₃ / dimethylformamide / 48 h / 20 °C

With sodium hydroxide; sodium hydrogencarbonate; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol016158l

Reference yield:

: 99-31-0
5-aminoisophthalic acid

: 363602-35-1
5-[(tert-butyloxycarbonyl)amino]-isophthalic acid mono allyl mono benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 98 percent / sodium hydroxide / H₂O; dioxane / 0 - 20 °C

2.1: NaHCO₃ / dimethylformamide

2.2: 34 percent / dimethylformamide / 24 h

3.1: 81 percent / NaHCO₃ / dimethylformamide / 48 h / 20 °C

With sodium hydroxide; sodium hydrogencarbonate; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol016158l