C₂₆H₂₂ClNO₃

Base Information

Chemical Name:C₂₆H₂₂ClNO₃
CAS No.:1278540-59-2
Molecular Formula:C₂₆H₂₂ClNO₃
Molecular Weight:431.919
Hs Code.:

C<sub>26</sub>H<sub>22</sub>ClNO<sub>3</sub>

Synonyms:C₂₆H₂₂ClNO₃

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Chemical Property of C₂₆H₂₂ClNO₃

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Technology Process of C₂₆H₂₂ClNO₃

There total 2 articles about C₂₆H₂₂ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1278540-62-7
C₁₉H₁₉NO₂

: 122-01-0
4-chloro-benzoyl chloride

: 1278540-59-2
C₂₆H₂₂ClNO₃

Guidance literature:: C₁₉H₁₉NO₂; With potassium tert-butylate; In tetrahydrofuran; at -40 ℃; for 1h;

4-chloro-benzoyl chloride; In tetrahydrofuran; for 3h;
DOI:10.1021/jm301084z

Reference yield:

: 1192805-45-0
N-p-toluenesulfonyl-2-ethylindole

: 1278540-59-2
C₂₆H₂₂ClNO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / methanol / 4 h / Reflux

2.1: n-butyllithium; zinc(II) chloride / tetrahydrofuran; hexane / 1.83 h / 0 - 20 °C

2.2: 18 h

3.1: potassium tert-butylate / tetrahydrofuran / 1 h / -40 °C

3.2: 3 h

With n-butyllithium; potassium tert-butylate; potassium hydroxide; zinc(II) chloride; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/jm301084z