bis(1,3-dichloro-2-azulenyl)phenylstibine

Base Information

Chemical Name:bis(1,3-dichloro-2-azulenyl)phenylstibine
CAS No.:827347-33-1
Molecular Formula:C₂₆H₁₅Cl₄Sb
Molecular Weight:590.967
Hs Code.:

Synonyms:bis(1,3-dichloro-2-azulenyl)phenylstibine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(1,3-dichloro-2-azulenyl)phenylstibine

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Technology Process of bis(1,3-dichloro-2-azulenyl)phenylstibine

There total 1 articles about bis(1,3-dichloro-2-azulenyl)phenylstibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 14658-94-7
1,3-dichloroazulene

: 5035-52-9
dichlorophenylstibine

: 827347-33-1
bis(1,3-dichloro-2-azulenyl)phenylstibine

Guidance literature:: With lithium 2,2,6,6-tetramethylpiperidide; In tetrahydrofuran; under Ar atm. to soln. lithium 2,2,6,6-tetramethylpiperidide in THF at -70°C soln. 1,3-dichloroazulene was added, soln. PhSbCl2 in THF was added and stirred for 5 min; elem. anal.;
DOI:10.1021/om040053f

Reference yield: 93.0%

: 13709-36-9
xenon difluoride

: 827347-33-1
bis(1,3-dichloro-2-azulenyl)phenylstibine

: 827347-41-1
bis(1,3-dichloro-2-azulenyl)phenylantimony difluoride

Guidance literature:: In tetrahydrofuran; under Ar atm. to soln. Sb compound in THF XeF2 was added at 0°C, react. mixt. was stirred for 3 h; soln. was evapd., residue was crystd. from MeOH; elem. anal.;
DOI:10.1021/om040053f