{Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2)

Base Information

Chemical Name:{Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2)
CAS No.:114220-88-1
Molecular Formula:C₈₀H₁₁₈N₂O₈Ta₂
Molecular Weight:1597.72
Hs Code.:

Synonyms:{Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2)

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Chemical Property of {Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2)

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Technology Process of {Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2)

There total 1 articles about {Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 90130-65-7
{TaCl3(THF)2}2(μ-N2)

: LiO-2,6-C6H3-i-Pr2*Et2O

: 114220-88-1
{Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2)

Guidance literature:: In tetrahydrofuran; diethyl ether; byproducts: LiCl; Li(O-2,6-C6H3-i-Pr2)*Et2O was added as a solid to {TaCl3(THF)2}2(μ-N2) dissolved in a mixt. of ether and THF, and the soln. was stirred at room temp. for 4 h. The soln. turned yellow and a white ppt. (LICl) was observed.; The mixt. was filtered, and the solvent was removed in vac., leaving a yellow oil. The oil was dissolved in ether, and the soln. was cooled to -30°C to yield yellow crystals.;

Reference yield: 83.0%

: 114220-88-1
{Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2)

: 100-52-7
benzaldehyde

: Ta(O)(O-2,6-C₆H₃-i-Pr₂)3

: 588-68-1,28867-76-7,65997-87-7,65997-88-8
benzaldehyde azine

Guidance literature:: In benzene-d6; {Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2) was dissolved in benzene-d6, and benzaldehyde was added.; The react. was monitored by (1)H-NMR spectroscopy at 25 and 65°C.;

Reference yield:

: 110-86-1
pyridine

: 114220-88-1
{Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2)

: 114198-86-6
{Ta(O-2,6-C6H3-i-Pr2)3(py)2}(μ-N2)

Guidance literature:: In diethyl ether; Pyridine was added to a soln. of {Ta(O-2,6-C6H3-i-Pr2)3(THF)}2(μ-N2) in ether at room temp. The soln. was stirred for 1 h, during which time the color changed from yellow to orange.; The solvent was removed in vac. and the resulting residue recrystd. from ether at -30°C. Elem.anal.;