(1S,2S,5R)-1-(4-methoxybenzoyl)-2-(1-methylethyl)-5-methylcyclohexan-1-ol

Base Information

Chemical Name:(1S,2S,5R)-1-(4-methoxybenzoyl)-2-(1-methylethyl)-5-methylcyclohexan-1-ol
CAS No.:50465-27-5
Molecular Formula:C₁₈H₂₆O₃
Molecular Weight:290.403
Hs Code.:

Synonyms:(1S,2S,5R)-1-(4-methoxybenzoyl)-2-(1-methylethyl)-5-methylcyclohexan-1-ol

Suppliers and Price of (1S,2S,5R)-1-(4-methoxybenzoyl)-2-(1-methylethyl)-5-methylcyclohexan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,5R)-1-(4-methoxybenzoyl)-2-(1-methylethyl)-5-methylcyclohexan-1-ol

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Technology Process of (1S,2S,5R)-1-(4-methoxybenzoyl)-2-(1-methylethyl)-5-methylcyclohexan-1-ol

There total 18 articles about (1S,2S,5R)-1-(4-methoxybenzoyl)-2-(1-methylethyl)-5-methylcyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2216-51-5
(-)-menthol

: 100-09-4
4-methoxybenzoic acid

: 50465-27-5
(1S,2S,5R)-1-(4-methoxybenzoyl)-2-(1-methylethyl)-5-methylcyclohexan-1-ol

Guidance literature:: With tributylphosphine; diamide; In benzene; at 60 ℃; for 24h;
DOI:10.1016/0040-4039(95)00299-R

Reference yield: 92.0%

: 2216-51-5
(-)-menthol

: 121-98-2
methyl 4-methoxybenzoate

: 50465-27-5,50465-29-7,50465-33-3,50465-35-5,58580-86-2,94003-48-2,4951-49-9
(1R,2S,2S,5S)-2-isopropyl-5-methylcyclohexyl-1-(4'-methoxybenzoate)

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; for 18h; Ambient temperature;
DOI:10.1039/c39860000695

Reference yield: 73.0%

: 201230-82-2
carbon monoxide

: 2216-51-5
(-)-menthol

: 459-64-3
4-methoxybenzenediazonium tetrafluoroborate

: 50465-27-5,50465-29-7,50465-33-3,50465-35-5,58580-86-2,94003-48-2,4951-49-9
(1R,2S,2S,5S)-2-isopropyl-5-methylcyclohexyl-1-(4'-methoxybenzoate)

Guidance literature:: With fluorescein free acid; In acetonitrile; at 20 ℃; for 21h; under 60804.1 Torr; Autoclave; Irradiation;
DOI:10.1002/anie.201408837