3-Ethoxy-4-methoxybenzenethiol

Base Information

Chemical Name:3-Ethoxy-4-methoxybenzenethiol
CAS No.:111424-64-7
Molecular Formula:C₉H₁₂O₂S
Molecular Weight:184.259
Hs Code.:

Synonyms:3-Ethoxy-4-methoxybenzenethiol

Suppliers and Price of 3-Ethoxy-4-methoxybenzenethiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 3-Ethoxy-4-methoxybenzenethiol

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Ethoxy-4-methoxybenzenethiol

There total 3 articles about 3-Ethoxy-4-methoxybenzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37942-01-1
5-bromo-2-methoxyphenol

: 111424-64-7
3-Ethoxy-4-methoxybenzenethiol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaOH / H₂O / 1.) room temp., 1 h; 2.) reflux, 40 min

2: 1.) Mg; 2.) S / 1.) THF, reflux, 30 min; 2.) room temp., 2 h

With sodium hydroxide; magnesium; In water;
DOI:10.1055/s-1987-27866

Reference yield:

: 25016-01-7
5-bromo-2-methoxybenzaldehyde

: 111424-64-7
3-Ethoxy-4-methoxybenzenethiol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 30percent peracetic acid; 2.) FeSO₄ / 1.) acetic acid, room temp., 16 h; 2.) H₂O, 20 min

2: 85 percent / NaOH / H₂O / 1.) room temp., 1 h; 2.) reflux, 40 min

3: 1.) Mg; 2.) S / 1.) THF, reflux, 30 min; 2.) room temp., 2 h

With peracetic acid; sodium hydroxide; iron(II) sulfate; magnesium; In water;
DOI:10.1055/s-1987-27866