4-BROMO-2-ETHOXY-1-METHOXYBENZENE

Base Information

Chemical Name:4-BROMO-2-ETHOXY-1-METHOXYBENZENE
CAS No.:52849-52-2
Molecular Formula:C9H11BrO2
Molecular Weight:231.089
Hs Code.:2909309090
Mol file:52849-52-2.mol

Synonyms:1-Bromo-3-ethoxy-4-methoxybenzene;4-Bromo-2-ethoxy-1-methoxybenzene;4-Bromo-2-ethoxyanisole;

Suppliers and Price of 4-BROMO-2-ETHOXY-1-METHOXYBENZENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Bromo-2-ethoxyanisole
500mg
$ 65.00

TRC
4-Bromo-2-ethoxyanisole
100mg
$ 45.00

Matrix Scientific
4-Bromo-2-ethoxy-1-methoxybenzene 98%
5g
$ 406.00

Crysdot
4-Bromo-2-ethoxy-1-methoxybenzene 98%
25g
$ 452.00

American Custom Chemicals Corporation
4-BROMO-2-ETHOXY-1-METHOXYBENZENE 95.00%
1G
$ 203.70

American Custom Chemicals Corporation
4-BROMO-2-ETHOXY-1-METHOXYBENZENE 95.00%
10G
$ 1479.56

Alichem
4-Bromo-2-ethoxy-1-methoxybenzene
25g
$ 478.80

AK Scientific
4-Bromo-2-ethoxy-1-methoxybenzene
25g
$ 691.00

Total 22 raw suppliers

Chemical Property of 4-BROMO-2-ETHOXY-1-METHOXYBENZENE

Chemical Property:

Vapor Pressure:0.031mmHg at 25°C
Refractive Index:1.523
Boiling Point:252.08 °C at 760 mmHg
Flash Point:100.607 °C
PSA：18.46000
Density:1.358 g/cm³
LogP:2.85640
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-2-ethoxyanisole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-BROMO-2-ETHOXY-1-METHOXYBENZENE

There total 7 articles about 4-BROMO-2-ETHOXY-1-METHOXYBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 37942-01-1
5-bromo-2-methoxyphenol

: 75-03-6
ethyl iodide

: 52849-52-2
1-Bromo-3-ethoxy-4-methoxybenzene

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 10.5h;

Reference yield: 85.0%

: 64-67-5
diethyl sulfate

: 37942-01-1
5-bromo-2-methoxyphenol

: 52849-52-2
1-Bromo-3-ethoxy-4-methoxybenzene

Guidance literature:: With sodium hydroxide; In water; 1.) room temp., 1 h; 2.) reflux, 40 min;
DOI:10.1055/s-1987-27866

Reference yield:

: 66037-04-5
1-acetoxy-5-bromo-2-methoxybenzene

: 52849-52-2
1-Bromo-3-ethoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / methanol / 3 h / 70 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide; tetrahydrofuran / 10.5 h / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.9b01513