1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate

Base Information

Chemical Name:1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate
CAS No.:115892-39-2
Molecular Formula:CH₃O₄S*C₂₄H₂₂N₃O₃
Molecular Weight:511.555
Hs Code.:

Synonyms:1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate

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Chemical Property of 1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate

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Technology Process of 1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate

There total 5 articles about 1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 77-78-1
dimethyl sulfate

: 115892-37-0
1-phenyl-3-(2-pyridylethyl)-4-acetoxy-1,8-naphthyridin-2(1H)-one

: 115892-39-2
1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate

Guidance literature:: In benzene; for 1.5h; Heating;
DOI:10.1021/jm00119a010

Reference yield:

: 40134-18-7
methyl 2-chloropyridine-3-carboxylate

: 115892-39-2
1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent

2: 86 percent / potassium tert-butoxide / 1.) 0.25 h, 2.) heating, 4 h

3: 75 percent / benzene / 24 h / Heating

4: 86 percent / benzene / 1.5 h / Heating

With potassium tert-butylate; In benzene;
DOI:10.1021/jm00119a010

Reference yield:

: 51269-84-2
methyl 2-phenylamino-nicotinate

: 115892-39-2
1-phenyl-3-(2-N-methylpyridinium)-4-acetoxy-1,8-naphthyridin-2(1H)-one methyl sulfate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / potassium tert-butoxide / 1.) 0.25 h, 2.) heating, 4 h

2: 75 percent / benzene / 24 h / Heating

3: 86 percent / benzene / 1.5 h / Heating

With potassium tert-butylate; In benzene;
DOI:10.1021/jm00119a010