5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

Base Information

• Chemical Name: 5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide
• CAS No.: 120344-69-6
• Molecular Formula: Br*C₂₅H₂₀N₃O₄S₂
• Molecular Weight: 570.487

Synonyms:5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

Chemical Property of 5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

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Technology Process of 5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide

There total 3 articles about 5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-Nitrophenacyl bromide (99-81-0) + 4-(p-Methoxybenzylidene)amino-3-phenylthiazoline-2(3H)-thione (23149-96-4) → 5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide (120344-69-6)

Guidance literature:

With acetic acid; In isopropyl alcohol; 1.) reflux, 5 min, 2.) room temp., 30 min;

DOI:10.1055/s-1988-27691

Reference yield:

3-amino-4-phenylthiazoline-2(3H)-thione (5316-81-4) → 5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide (120344-69-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / NaOAc / aq. ethanol / 0.5 h / Heating

2: 70 percent / HOAc / propan-2-ol / 1.) reflux, 5 min, 2.) room temp., 30 min

With sodium acetate; acetic acid; In ethanol; isopropyl alcohol;

DOI:10.1055/s-1988-27691

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → 5-(4-Methoxy-phenyl)-6-(4-nitro-benzoyl)-3-phenyl-5,6-dihydro-4H-1,7-dithia-4-aza-3a-azonia-indene; bromide (120344-69-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / NaOAc / aq. ethanol / 0.5 h / Heating

2: 70 percent / HOAc / propan-2-ol / 1.) reflux, 5 min, 2.) room temp., 30 min

With sodium acetate; acetic acid; In ethanol; isopropyl alcohol;

DOI:10.1055/s-1988-27691

upstream raw materials:

4-Nitrophenacyl bromide

4-(p-Methoxybenzylidene)amino-3-phenylthiazoline-2(3H)-thione

3-amino-4-phenylthiazoline-2(3H)-thione

4-methoxy-benzaldehyde

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