di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate

Base Information

Chemical Name:di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate
CAS No.:1334542-41-4
Molecular Formula:C₃₁H₄₇NO₅Si
Molecular Weight:541.803
Hs Code.:

Synonyms:di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate

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Chemical Property of di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate

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Technology Process of di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate

There total 4 articles about di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51779-32-9
iminodicarboxylic acid di-tert-butyl ester

: 154912-70-6
(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutan-1-ol

: 1334542-41-4
di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In toluene; at 20 ℃; for 15.5h;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1334542-41-4
di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / dichloromethane / 24 h / 20 °C / Cooling with ice

2: diisobutylaluminium hydride / tetrahydrofuran / 2.08 h / -78 °C / Inert atmosphere

3: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 15.5 h / 20 °C

With 1H-imidazole; tributylphosphine; diisobutylaluminium hydride; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 147915-53-5
(S)-methyl-3-hydroxy-2-methylpropanoate

: 1334542-41-4
di-tert-butyl [(3R)-4-{[tert-butyl(diphenyl)silyl]oxy}-3-methylbutyl]imidodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / dichloromethane / 24 h / 20 °C / Cooling with ice

2: diisobutylaluminium hydride / tetrahydrofuran / 2.08 h / -78 °C / Inert atmosphere

3: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 15.5 h / 20 °C

With 1H-imidazole; tributylphosphine; diisobutylaluminium hydride; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; dichloromethane; toluene;