1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene

Base Information

Chemical Name:1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene
CAS No.:1459808-93-5
Molecular Formula:C₁₆H₁₂F₃N₃S
Molecular Weight:335.353
Hs Code.:

Synonyms:1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene

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Chemical Property of 1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene

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Technology Process of 1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene

There total 5 articles about 1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1459808-92-4
C₁₅H₁₄F₃N₃

: 102368-13-8
1,1'-Thiocarbonyldi-2(1H)-pyridone

: 1459808-93-5
1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene

Guidance literature:: In dichloromethane; at 20 ℃; for 16h;
DOI:10.1002/anie.201302530

Reference yield:

: 13472-00-9
p-Aminophenethylamine

: 1459808-93-5
1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene

Guidance literature:: Multi-step reaction with 5 steps

1: dmap / tetrahydrofuran / 16 h / 20 °C

2: Oxone / dichloromethane; ethanol; water / 12 h / 20 °C

3: acetic acid / dimethyl sulfoxide / 24 h / 20 °C

4: hydrogenchloride / 1,4-dioxane; water / 16 h / 20 °C

5: dichloromethane / 16 h / 20 °C

With hydrogenchloride; dmap; Oxone; acetic acid; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/anie.201302530

Reference yield:

: 1459808-91-3
tert-butyl 4-((4-(trifluoromethyl)phenyl)diazenyl)phenethylcarbamate

: 1459808-93-5
1-(4-(2-isothiocyanatoethyl)phenyl)-2-(4-(trifluoromethyl)phenyl)diazene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; water / 16 h / 20 °C

2: dichloromethane / 16 h / 20 °C

With hydrogenchloride; In 1,4-dioxane; dichloromethane; water;
DOI:10.1002/anie.201302530