2-amino-3-benzylindazole

Base Information

Chemical Name:2-amino-3-benzylindazole
CAS No.:80749-49-1
Molecular Formula:C₁₄H₁₃N₃
Molecular Weight:223.277
Hs Code.:

Synonyms:2-amino-3-benzylindazole

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Chemical Property of 2-amino-3-benzylindazole

Chemical Property:

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Technology Process of 2-amino-3-benzylindazole

There total 4 articles about 2-amino-3-benzylindazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26211-73-4
(2-methyl-1H-indol-3-yl)phenylmethanone

: 80749-49-1
2-amino-3-benzylindazole

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) BH₃*SMe₂, 2.) CH₃OH / 1.) THF, 0 deg C, 2 h; r.t., 2 h, 2.) THF, 1 h, reflux

2: 80 percent / O₃/O₂ / ethyl acetate / 14 h

3: 67 percent / 5M HCl / ethanol / 3 h / Heating

4: 1.) NaNO₂, 10M HCl, 2.) NaN₃ / 1.) H₂O, 0 deg C, 30 min, 2.) H₂O, 10 min

5: 75 percent / NH₂NH₂*H₂O, CH₃COOH / ethanol / 15 h / Heating

6: 1.) NaOH, 2.) NH₂OSO₃H / 1.) EtOH, H₂O, 50 deg C, 2.) EtOH, H₂O, 50-55 deg C, 30 min

With hydrogenchloride; methanol; sodium hydroxide; sodium azide; dimethylsulfide borane complex; oxygen; ozone; hydrazine hydrate; acetic acid; hydroxylamine-O-sulfonic acid; sodium nitrite; In ethanol; ethyl acetate;

Reference yield:

: 19988-04-6
N-(2-(2-phenylacetyl)phenyl)acetamide

: 80749-49-1
2-amino-3-benzylindazole

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / 5M HCl / ethanol / 3 h / Heating

2: 1.) NaNO₂, 10M HCl, 2.) NaN₃ / 1.) H₂O, 0 deg C, 30 min, 2.) H₂O, 10 min

3: 75 percent / NH₂NH₂*H₂O, CH₃COOH / ethanol / 15 h / Heating

4: 1.) NaOH, 2.) NH₂OSO₃H / 1.) EtOH, H₂O, 50 deg C, 2.) EtOH, H₂O, 50-55 deg C, 30 min

With hydrogenchloride; sodium hydroxide; sodium azide; hydrazine hydrate; acetic acid; hydroxylamine-O-sulfonic acid; sodium nitrite; In ethanol;

Reference yield:

: 80749-42-4
2-azidophenyl benzyl ketone

: 80749-49-1
2-amino-3-benzylindazole

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NH₂NH₂*H₂O, CH₃COOH / ethanol / 15 h / Heating

2: 1.) NaOH, 2.) NH₂OSO₃H / 1.) EtOH, H₂O, 50 deg C, 2.) EtOH, H₂O, 50-55 deg C, 30 min

With sodium hydroxide; hydrazine hydrate; acetic acid; hydroxylamine-O-sulfonic acid; In ethanol;