2-azidophenyl benzyl ketone

Base Information

Chemical Name:2-azidophenyl benzyl ketone
CAS No.:80749-42-4
Molecular Formula:C₁₄H₁₁N₃O
Molecular Weight:237.261
Hs Code.:

Synonyms:2-azidophenyl benzyl ketone

Suppliers and Price of 2-azidophenyl benzyl ketone

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Chemical Property of 2-azidophenyl benzyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2-azidophenyl benzyl ketone

There total 4 articles about 2-azidophenyl benzyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-20-5
2-methyl-1H-indole

: 80749-42-4
2-azidophenyl benzyl ketone

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) EtMgBr / 1.) Et₂O, 2 h, reflux; 2.) Et₂O, 30 min

2: 1.) BH₃*SMe₂, 2.) CH₃OH / 1.) THF, 0 deg C, 2 h; r.t., 2 h, 2.) THF, 1 h, reflux

3: 80 percent / O₃/O₂ / ethyl acetate / 14 h

4: 67 percent / 5M HCl / ethanol / 3 h / Heating

5: 1.) NaNO₂, 10M HCl, 2.) NaN₃ / 1.) H₂O, 0 deg C, 30 min, 2.) H₂O, 10 min

With hydrogenchloride; methanol; sodium azide; dimethylsulfide borane complex; ethylmagnesium bromide; oxygen; ozone; sodium nitrite; In ethanol; ethyl acetate;

Reference yield:

: 26211-73-4
(2-methyl-1H-indol-3-yl)phenylmethanone

: 80749-42-4
2-azidophenyl benzyl ketone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) BH₃*SMe₂, 2.) CH₃OH / 1.) THF, 0 deg C, 2 h; r.t., 2 h, 2.) THF, 1 h, reflux

2: 80 percent / O₃/O₂ / ethyl acetate / 14 h

3: 67 percent / 5M HCl / ethanol / 3 h / Heating

4: 1.) NaNO₂, 10M HCl, 2.) NaN₃ / 1.) H₂O, 0 deg C, 30 min, 2.) H₂O, 10 min

With hydrogenchloride; methanol; sodium azide; dimethylsulfide borane complex; oxygen; ozone; sodium nitrite; In ethanol; ethyl acetate;

Reference yield:

: 19988-04-6
N-(2-(2-phenylacetyl)phenyl)acetamide

: 80749-42-4
2-azidophenyl benzyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / 5M HCl / ethanol / 3 h / Heating

2: 1.) NaNO₂, 10M HCl, 2.) NaN₃ / 1.) H₂O, 0 deg C, 30 min, 2.) H₂O, 10 min

With hydrogenchloride; sodium azide; sodium nitrite; In ethanol;