3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione

Base Information

Chemical Name:3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione
CAS No.:1615201-99-4
Molecular Formula:C₁₇H₁₄Cl₂O₃
Molecular Weight:337.202
Hs Code.:

Synonyms:3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione

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Chemical Property of 3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione

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Technology Process of 3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione

There total 11 articles about 3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1615212-11-7
3-(2-chloro-4-ethynyl-6-methoxyphenyl)-2-methoxybicyclo[3.2.1]oct-2-en-4-one

: 1615201-99-4
3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione

Guidance literature:: 3-(2-chloro-4-ethynyl-6-methoxyphenyl)-2-methoxybicyclo[3.2.1]oct-2-en-4-one; With tetrachloromethane; tetrabutyl ammonium fluoride; potassium carbonate; at 20 ℃;

With hydrogenchloride; In water; at 60 ℃; for 3h;

Reference yield:

: 1615202-04-4
3-(2-chloro-4-ethynyl-6-methoxyphenyl)bicyclo[3.2.1]octane-2,4-dione

: 1615201-99-4
3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 16 h / 20 °C

2.1: tetrachloromethane; potassium carbonate; tetrabutyl ammonium fluoride / 20 °C

2.2: 3 h / 60 °C

With tetrachloromethane; tetrabutyl ammonium fluoride; potassium carbonate; In acetone;

Reference yield:

: 1615212-15-1
3-[2-chloro-6-methoxy-4-(2-trimethylsilylethynyl)phenyl]bicyclo[3.2.1 ]octane-2,4-dione

: 1615201-99-4
3-[2-chloro-4-(2-chloroethynyl)-6-methoxyphenyl]bicyclo[3.2.1]octane-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / methanol / 2 h

2.1: potassium carbonate / acetone / 16 h / 20 °C

3.1: tetrachloromethane; potassium carbonate; tetrabutyl ammonium fluoride / 20 °C

3.2: 3 h / 60 °C

With tetrachloromethane; tetrabutyl ammonium fluoride; potassium carbonate; In methanol; acetone;