methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate

Base Information

Chemical Name:methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate
CAS No.:1452823-71-0
Molecular Formula:C₁₈H₁₉NO₅
Molecular Weight:329.353
Hs Code.:

Synonyms:methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate

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Chemical Property of methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate

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Technology Process of methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate

There total 1 articles about methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 54555-84-9
benzyl iodoethyl ether

: 30095-98-8
methyl (2-nitrophenyl)acetate

: 1452823-71-0
methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;
DOI:10.1002/anie.201209970

Reference yield: 91.0%

: 1452823-71-0
methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate

: 1452823-72-1
potassium 4-(benzyloxy)2-(2-nitrophenyl)butanoate

Guidance literature:: methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate; With potassium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=4 - 5; Inert atmosphere;

With potassium tert-butylate; In ethanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201209970

Reference yield:

: 1452823-71-0
methyl 4-(benzyloxy)-2-(2-nitrophenyl)butanoate

: 1452823-99-2
(E)-1-(3-(benzyloxy)prop-1-en-1-yl)-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / tetrahydrofuran; methanol; water / 20 °C / Inert atmosphere

1.2: pH 4 - 5 / Inert atmosphere

1.3: 1 h / 20 °C / Inert atmosphere

2.1: bis(η3-allyl-μ-chloropalladium(II)); XPhos / diethylene glycol dimethyl ether / 2 h / 100 °C / Inert atmosphere

With bis(η3-allyl-μ-chloropalladium(II)); potassium hydroxide; XPhos; In tetrahydrofuran; methanol; diethylene glycol dimethyl ether; water;
DOI:10.1002/anie.201209970