dimethyl(o-anisyl)phosphine sulfide

Base Information

Chemical Name:dimethyl(o-anisyl)phosphine sulfide
CAS No.:42337-00-8
Molecular Formula:C₉H₁₃OPS
Molecular Weight:200.241
Hs Code.:

Synonyms:dimethyl(o-anisyl)phosphine sulfide

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Chemical Property of dimethyl(o-anisyl)phosphine sulfide

Chemical Property:

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Technology Process of dimethyl(o-anisyl)phosphine sulfide

There total 2 articles about dimethyl(o-anisyl)phosphine sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 589-57-1
diethyl phosphorylchloridite

: 75-16-1
methylmagnesium bromide

: 480438-46-8
Grignard reagent from 2-methoxybenzyl chloride

: 42337-00-8
dimethyl(o-anisyl)phosphine sulfide

Guidance literature:: diethyl phosphorylchloridite; Grignard reagent from 2-methoxybenzyl chloride; In tetrahydrofuran; at -78 - 20 ℃; Schlenk technique; Inert atmosphere;

methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 21h; Schlenk technique; Inert atmosphere;

With sulfur; In tetrahydrofuran; diethyl ether; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.joc.7b01767

Reference yield:

: 42337-00-8
dimethyl(o-anisyl)phosphine sulfide

Guidance literature:: With sulfur;

Reference yield: 81.0%

: 6940-78-9
4-chlorobutyl bromide

: 42337-00-8
dimethyl(o-anisyl)phosphine sulfide

: (5-chloropentyl)(methyl)(o-anisyl)phosphine sulfide

Guidance literature:: dimethyl(o-anisyl)phosphine sulfide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere; Schlenk technique;

4-chlorobutyl bromide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.joc.7b01767