methyl benzoyl formate phenylhydrazone

Base Information

• Chemical Name: methyl benzoyl formate phenylhydrazone
• CAS No.: 23102-13-8
• Molecular Formula: C₁₅H₁₄N₂O₂
• Molecular Weight: 254.288

Synonyms:methyl benzoyl formate phenylhydrazone

Chemical Property of methyl benzoyl formate phenylhydrazone

Chemical Property:

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Technology Process of methyl benzoyl formate phenylhydrazone

There total 6 articles about methyl benzoyl formate phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methyl 2-oxo-2-phenylacetate (15206-55-0) + phenylhydrazine (100-63-0) → methyl benzoyl formate phenylhydrazone (23102-13-8)

Guidance literature:

In ethylene glycol; for 0.1h; Heating;

DOI:10.1021/jo981516s

Reference yield: 15.0%

Methyl azido-(phenylhydrazono)-acetate (93831-03-9) → biphenyl (92-52-4,1594-86-1) + 1-phenyl-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-45-1) + methyl α-aminoglyoxylate phenylhydrazone (74669-09-3) + methyl benzoyl formate phenylhydrazone (23102-13-8)

Guidance literature:

In benzene; for 4h; Heating;

Reference yield: 2.0%

Methyl azido-(phenylhydrazono)-acetate (93831-03-9) → methyl 1-phenyl-1H-1,2,4-triazole-3-carboxylate (57226-96-7) + 1-phenyl-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-45-1) + methyl α-aminoglyoxylate phenylhydrazone (74669-09-3) + methyl benzoyl formate phenylhydrazone (23102-13-8)

Guidance literature:

In 1,4-dioxane; for 2h; Further byproducts given; Heating; benzene, 4 h; ethanol, 3 h;

upstream raw materials:

methyl 2-oxo-2-phenylacetate

Methyl azido-(phenylhydrazono)-acetate

phenylhydrazine

(RS)-methyl mandelate

Downstream raw materials:

phenylglycine methyl ester

methyl 2-acetamido-2-phenylacetate

methyl 1-phenyl-1H-indazole-3-carboxylate

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