erythro (2R,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol

Base Information

• Chemical Name: erythro (2R,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol
• CAS No.: 130718-70-6
• Molecular Formula: C₂₄H₂₆O₃S₂
• Molecular Weight: 426.601

Synonyms:erythro (2R,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol

Chemical Property of erythro (2R,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol

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Technology Process of erythro (2R,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol

There total 9 articles about erythro (2R,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-hydroxy-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propan-2-one (130796-22-4) → erythro 3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol (130718-70-6,130718-72-8,130796-24-6)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 0.666667h; Ambient temperature;

Reference yield: 82.0%

(R)-3-hydroxy-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propan-2-one (130718-67-1) → erythro (2R,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol (130718-70-6)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 0.666667h; Ambient temperature;

Reference yield: 48.0%

(R)-3-hydroxy-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propan-2-one (130718-67-1) → erythro (2R,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol (130718-70-6) + threo (2S,3R)-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propane-2,3-diol (130718-72-8)

Guidance literature:

With diisobutylaluminium hydride; In diethyl ether; toluene; at -78 ℃; for 1h;

upstream raw materials:

3-hydroxy-3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)propan-2-one

methyl 2-(4-methoxyphenyl)-2-(trimethylsilyloxy)acetate

methyl 2-hydroxy-2-(4-methoxyphenyl)acetate

3-(4-methoxyphenyl)-1,1-bis(p-tolylthio)-3-(trimethylsilyloxy)propan-2-one

Downstream raw materials:

methyl (4R,5R)-cis-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carboxylate

methyl (4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carboxylate

(-)-(2R,3R)-methyl-2,3-dihydroxy-3-para-methoxyphenyl-propanoate

(2S,3R)-(-)-methyl 2,3-dihydroxy-3-(p-methoxyphenyl)propionate

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