methyl (2S)-2-[(4-methylphenylsulfonyl)-(2-butyn-1-yl)-amino]-3-butenoate

Base Information

Chemical Name:methyl (2S)-2-[(4-methylphenylsulfonyl)-(2-butyn-1-yl)-amino]-3-butenoate
CAS No.:1190409-85-8
Molecular Formula:C₁₆H₁₉NO₄S
Molecular Weight:321.397
Hs Code.:

Synonyms:methyl (2S)-2-[(4-methylphenylsulfonyl)-(2-butyn-1-yl)-amino]-3-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2S)-2-[(4-methylphenylsulfonyl)-(2-butyn-1-yl)-amino]-3-butenoate

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Technology Process of methyl (2S)-2-[(4-methylphenylsulfonyl)-(2-butyn-1-yl)-amino]-3-butenoate

There total 1 articles about methyl (2S)-2-[(4-methylphenylsulfonyl)-(2-butyn-1-yl)-amino]-3-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1190409-87-0
methyl (2S)-2-[[(4-methylphenyl)sulfonyl]-(2-butyn-1-yl)-amino]-4-(phenylseleno)butanoate

: 1190409-85-8
methyl (2S)-2-[(4-methylphenylsulfonyl)-(2-butyn-1-yl)-amino]-3-butenoate

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; for 16.5h;
DOI:10.1021/ja9063475

Reference yield:

: 201230-82-2
carbon monoxide

: 1190409-85-8
methyl (2S)-2-[(4-methylphenylsulfonyl)-(2-butyn-1-yl)-amino]-3-butenoate

: 766-77-8
Dimethylphenylsilane

: 1190409-84-7
(2S,3S,4E)-1-[(4-methylphenyl)sulfonyl]-2-methoxycarbonyl-4-[1-(phenyldimethylsilyl)ethylidene]-3-pyrrolidineacetaldehyde

: (4E)-1-[(4-methylphenyl)sulfonyl]-2-methoxycarbonyl-4-[(phenyldimethylsilyl)ethylidene]-3-pyrrolidineacetaldehyde

Guidance literature:: With acetylacetonatodicarbonylrhodium(l); In toluene; at 120 ℃; for 12h; under 25858.1 Torr; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ja9063475