2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate

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Chemical Name:2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate
CAS No.:1310327-46-8
Molecular Formula:C₂F₃O₂*C₂₇H₂₈N₃O₄S
Molecular Weight:603.619
Hs Code.:

Synonyms:2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate

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Chemical Property of 2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate

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Technology Process of 2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate

There total 6 articles about 2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 1310327-44-6
4-(2-((1E,3E)-4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazol-3-ium-3-yl)butanoate trifluoroacetate

: 1310327-46-8
2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate

Guidance literature:: With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2011.03.045

Reference yield:

: 120-75-2
2-Methylbenzothiazole

: 1310327-46-8
2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 72 h / 110 °C

2: pyridine / methanol / 18 h / Reflux

3: lithium hydroxide / tetrahydrofuran; ethanol; water / 3 h / 20 °C

4: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 0 - 20 °C

With pyridine; dicyclohexyl-carbodiimide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.03.045

Reference yield:

: 1310327-41-3
3-(4-methoxy-4-oxobutyl)-2-methylbenzo[d]thiazol-3-ium bromide

: 1310327-46-8
2-(4-(4-(dimethylamino)phenyl)buta-1,3-dienyl)-3-(4-(2,5-dioxopyrrolidin-1-yloxy)-4-oxobutyl)benzo[d]thiazol-3-ium trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / methanol / 18 h / Reflux

2: lithium hydroxide / tetrahydrofuran; ethanol; water / 3 h / 20 °C

3: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 0 - 20 °C

With pyridine; dicyclohexyl-carbodiimide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.03.045