4-methyl-N-(pyrene-1-ylmethylene)aniline

Base Information

• Chemical Name: 4-methyl-N-(pyrene-1-ylmethylene)aniline
• CAS No.: 1204704-26-6
• Molecular Formula: C₂₄H₁₇N
• Molecular Weight: 319.406
• Mol file: 1204704-26-6.mol

Synonyms:4-methyl-N-(pyrene-1-ylmethylene)aniline

Chemical Property of 4-methyl-N-(pyrene-1-ylmethylene)aniline

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-methyl-N-(pyrene-1-ylmethylene)aniline

There total 1 articles about 4-methyl-N-(pyrene-1-ylmethylene)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

pyrene-1-aldehyde (3029-19-4) + p-toluidine (106-49-0,12221-03-3) → 4-methyl-N-(pyrene-1-ylmethylene)aniline (1204704-26-6)

Guidance literature:

In methanol; at 120 ℃; Microwave irradiation; Sealed vessel; Inert atmosphere;

DOI:10.1016/j.jorganchem.2009.09.030

Reference yield: 79.0%

diphenyl hydrogen phosphite (4712-55-4) + 4-methyl-N-(pyrene-1-ylmethylene)aniline (1204704-26-6) → diphenyl N-(4-methylphenyl)amino(pyren-1-yl)methylphosphonate

Guidance literature:

In dichloromethane; at 20 ℃; for 24h;

DOI:10.3390/molecules21070936

Reference yield: 68.0%

4-methyl-N-(pyrene-1-ylmethylene)aniline (1204704-26-6) + mercury(II) diacetate (1600-27-7) → HgCl(4-methyl-N-(pyrene-1-ylmethylene)aniline)

Guidance literature:

With LiCl; In methanol; (N2); Schiff base and Hg acetate stirred (24 h) together in refluxing MeOH, mixt. cooled, LiCl in hot MeOH added under stirring; ppt. filtered, washed (Et2O), dried, solid extd. by hexane via G-4 soxlet frit, recrystn. (CHCl3-MeOH, 1:1);

DOI:10.1016/j.jorganchem.2009.09.030

upstream raw materials:

pyrene-1-aldehyde

p-toluidine

Downstream raw materials:

C₃₀H₂₁Cl₂NTe

C₃₁H₂₃Cl₂NTe

C₃₁H₂₃Cl₂NOTe

C₃₃H₂₇Cl₂NTe