(1,3-dimethyl-1H-imidazol-3-ium-2-yl)(4-methoxyphenyl)dihydroborate

Base Information

Chemical Name:(1,3-dimethyl-1H-imidazol-3-ium-2-yl)(4-methoxyphenyl)dihydroborate
CAS No.:1250377-22-0
Molecular Formula:C₁₂H₁₇BN₂O
Molecular Weight:216.091
Hs Code.:

Synonyms:(1,3-dimethyl-1H-imidazol-3-ium-2-yl)(4-methoxyphenyl)dihydroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1,3-dimethyl-1H-imidazol-3-ium-2-yl)(4-methoxyphenyl)dihydroborate

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Technology Process of (1,3-dimethyl-1H-imidazol-3-ium-2-yl)(4-methoxyphenyl)dihydroborate

There total 2 articles about (1,3-dimethyl-1H-imidazol-3-ium-2-yl)(4-methoxyphenyl)dihydroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 15237-67-9
4-methoxyphenylborane pyridine complex

: 4333-62-4
1,3-dimethylimidazolim iodide

: 1250377-22-0
(1,3-dimethyl-1H-imidazol-3-ium-2-yl)(4-methoxyphenyl)dihydroborate

Guidance literature:: 1,3-dimethylimidazolim iodide; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h;

4-methoxyphenylborane pyridine complex; In tetrahydrofuran; at 20 ℃; Reflux;
DOI:10.1021/jo101301d

Reference yield:

: 1211417-77-4
(1,3-dimethylimidazol-2-ylidene)borane

: 556812-41-0
4-methoxy-2-(trimethylsilyl)phenyl triflate

: 1250377-22-0
(1,3-dimethyl-1H-imidazol-3-ium-2-yl)(4-methoxyphenyl)dihydroborate

: (1,3-dimethyl-1H-imidazol-3-ium-2-yl)(3-methoxyphenyl)dihydroborate

Guidance literature:: With potassium fluoride; 18-crown-6 ether; In tetrahydrofuran; at 20 ℃; for 42h; Overall yield = 43 %; Overall yield = 18.7 mg; Inert atmosphere;
DOI:10.1002/anie.201408345