5-benzyl-2-isopropyl-3-(methoxycarbonyl)-5-(5,5-pentamethylene-1,3,4-pentatrien-2-yl)-4,5-dihydrofuran

Base Information

Chemical Name:5-benzyl-2-isopropyl-3-(methoxycarbonyl)-5-(5,5-pentamethylene-1,3,4-pentatrien-2-yl)-4,5-dihydrofuran
CAS No.:1225232-90-5
Molecular Formula:C₂₆H₃₂O₃
Molecular Weight:392.538
Hs Code.:

Synonyms:5-benzyl-2-isopropyl-3-(methoxycarbonyl)-5-(5,5-pentamethylene-1,3,4-pentatrien-2-yl)-4,5-dihydrofuran

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Chemical Property of 5-benzyl-2-isopropyl-3-(methoxycarbonyl)-5-(5,5-pentamethylene-1,3,4-pentatrien-2-yl)-4,5-dihydrofuran

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Technology Process of 5-benzyl-2-isopropyl-3-(methoxycarbonyl)-5-(5,5-pentamethylene-1,3,4-pentatrien-2-yl)-4,5-dihydrofuran

There total 1 articles about 5-benzyl-2-isopropyl-3-(methoxycarbonyl)-5-(5,5-pentamethylene-1,3,4-pentatrien-2-yl)-4,5-dihydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1225232-78-9
C₁₈H₂₂O₃

: 61699-43-2
methyl 1,1-pentamethyleneprop-2-ynyl carbonate

: 1225232-90-5
5-benzyl-2-isopropyl-3-(methoxycarbonyl)-5-(5,5-pentamethylene-1,3,4-pentatrien-2-yl)-4,5-dihydrofuran

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; for 1.25h; chemoselective reaction; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2010.02.030

Reference yield: 96.0%

: 201230-82-2
carbon monoxide

: 1225232-90-5
5-benzyl-2-isopropyl-3-(methoxycarbonyl)-5-(5,5-pentamethylene-1,3,4-pentatrien-2-yl)-4,5-dihydrofuran

: 1225232-94-9
4-(5-benzyl-2-isopropyl-3-(methoxycarbonyl)-4,5-dihydrofuran-5-yl)-2-(1-cyclohexylidene)cyclopent-3-enone

Guidance literature:: With di(rhodium)tetracarbonyl dichloride; In 1,2-dichloro-ethane; at 20 ℃; for 1h; under 760.051 Torr;
DOI:10.1016/j.tet.2010.02.030