N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride

Base Information

Chemical Name:N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride
CAS No.:1186481-74-2
Molecular Formula:C₃₈H₇₇N₂O₅*Cl
Molecular Weight:677.493
Hs Code.:

Synonyms:N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride

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Chemical Property of N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride

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Technology Process of N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride

There total 4 articles about N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1186481-76-4
N-2-[N'-(l, 3, 4, 5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium iodide

: 1186481-74-2
N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride

Guidance literature:: N-2-[N'-(l, 3, 4, 5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium iodide; With methanol; sodium methylate; at 20 ℃; for 3h; pH=~ 9;

In chloroform;

Reference yield:

: 77-95-2
D-(-)-quinic acid

: 1186481-74-2
N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: perchloric acid / 20 - 60 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 0.5 h / Cooling with ice

2.2: 20 °C

3.1: methanol; chloroform / 6 h / 20 °C

4.1: methanol; sodium methylate / 3 h / 20 °C / pH ~ 9

4.2: amberlyst A-26 chloride ion exchange resin

With methanol; perchloric acid; sodium methylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide;

Reference yield:

: 32469-24-2
(1R,3R,4R,5R)-(-)-quinic acid tetraacetate

: 1186481-74-2
N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecyl,N-methyl ammonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 0.5 h / Cooling with ice

1.2: 20 °C

2.1: methanol; chloroform / 6 h / 20 °C

3.1: methanol; sodium methylate / 3 h / 20 °C / pH ~ 9

3.2: amberlyst A-26 chloride ion exchange resin

With methanol; sodium methylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide;