N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecylamine

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Chemical Name:N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecylamine
CAS No.:1186481-75-3
Molecular Formula:C₄₅H₈₂N₂O₉
Molecular Weight:795.154
Hs Code.:

Synonyms:N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecylamine

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Chemical Property of N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecylamine

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Technology Process of N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecylamine

There total 2 articles about N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 32469-24-2
(1R,3R,4R,5R)-(-)-quinic acid tetraacetate

: N-aminoethyl-N,N-di-n-tetradecylamine

: 1186481-75-3
N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecylamine

Guidance literature:: (1R,3R,4R,5R)-(-)-quinic acid tetraacetate; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; for 0.5h; Cooling with ice;

N-aminoethyl-N,N-di-n-tetradecylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 77-95-2
D-(-)-quinic acid

: 1186481-75-3
N-2-[N'-(1,3,4,5-tetraacetoxycyclohexanecarbonyl)]aminoethyl-N,N-di-n-tetradecylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: perchloric acid / 20 - 60 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 0.5 h / Cooling with ice

2.2: 20 °C

With perchloric acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;