2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine

Base Information

Chemical Name:2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine
CAS No.:273217-00-8
Molecular Formula:C₃₄H₃₇NO₄S
Molecular Weight:555.738
Hs Code.:

Synonyms:2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine

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Chemical Property of 2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine

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Technology Process of 2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine

There total 1 articles about 2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 2,5-bis(hydroxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine

: 273217-00-8
2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃;

Reference yield: 39.0%

: 273217-00-8
2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine

: (1'R,2S,5S)-2,5-bis(benzyloxymethyl)-1-(1-phenylethyl)-pyrrolidine

: 272774-28-4
(1'R,2R,5R)-2,5-bis(benzyloxymethyl)-1-(1-phenylethyl)-pyrrolidine

Guidance literature:: With disodium hydrogenphosphate; sodium amalgam; In tetrahydrofuran; methanol; at 20 ℃;

Reference yield:

: 273217-00-8
2,5-bis(benzyloxymethyl)-1-((1R)-1-phenylethyl)-3-phenylsulfonylpyrrolidine

: 127221-54-9
trans-(2R,5R)-bis(benzyloxymethyl)-pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / Na₂HPO₄; 10 percent Na-Hg / tetrahydrofuran; methanol / 20 °C

2: 90 percent / H₂ / 20 percent Pd(OH)2/C / ethanol / 20 °C

With disodium hydrogenphosphate; sodium amalgam; hydrogen; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; 1: desulfonation / 2: Hydrogenolysis;