[Et₄N][Mo₂O₂(PhS)6(OMe)]

Base Information

Chemical Name:[Et₄N][Mo₂O₂(PhS)6(OMe)]
CAS No.:69609-04-7
Molecular Formula:C₈H₂₀N*C₃₇H₃₃Mo₂O₃S₆
Molecular Weight:1040.2
Hs Code.:

[Et<sub>4</sub>N][Mo<sub>2</sub>O<sub>2</sub>(PhS)6(OMe)]

Synonyms:[Et₄N][Mo₂O₂(PhS)6(OMe)]

Suppliers and Price of [Et₄N][Mo₂O₂(PhS)6(OMe)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Et₄N][Mo₂O₂(PhS)6(OMe)]

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Technology Process of [Et₄N][Mo₂O₂(PhS)6(OMe)]

There total 2 articles about [Et₄N][Mo₂O₂(PhS)6(OMe)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 16925-10-3
pyridinium tetrabromooxomolybdate(V)

: 71-91-0
tetraethylammonium bromide

: 882-33-7
diphenyldisulfane

: 69609-04-7
[Et₄N][Mo₂O₂(PhS)6(OMe)]

Guidance literature:: With sodium borohydride; In methanol; under N2 or Ar; recrystn. from MeCN/MeOH at 60°C;
DOI:10.1021/ja00398a013

Reference yield:

: 20529-42-4
oxotrischlorobis(tetrahydrofuran)molybdenum(V)

: 124-41-4
sodium methylate

: 108-98-5
thiophenol

: 69609-04-7
[Et₄N][Mo₂O₂(PhS)6(OMe)]

Guidance literature:: With Et₄NBr; In methanol; byproducts: NaCl; C6H5SH was dissol. in the soln. of CH3ONa, the soln. was added to the stirred soln. of Mo complex, after 1 h NaCl was filtered off, the soln. of Et4NBr was added under N2; the soln. was cooled to -10°C overnight, ppt. was filtered, washed with methanol, dried in vac., recrystd. by cooling from acetonitrile/methanol, elem. anal.;